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{������'. Phenacetin (C 10 H 13 NO 2), N- (4-Ethoxyphenyl)acetamide, is a drug that saw widespread application for nearly a century in many over-the-counter medications as a remedy for pain and fever. /Producer(Sub Systems, Inc.)/CreationDate(D:20200301123517+05'00')/ModDate(D:20200301123517+05'00')/Creator(Sub Systems, Inc.)
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CCOc1ccc(cc1[N+](=O) [O-])NC(=O)C Copy. Separating the Components of Your Mixture All unknown mixtures can be separated by either acid-base extraction or recrystallization. List of 1-Acetyl-p-phenetidin; 4 inverted exclamation marka-Ethoxyacetanilide; N-(4-Ethoxyphenyl)acetamide; p-Acetophenetidide; Acetophenetidin Active Pharmaceutical Ingredient (API) suppliers/manufacturers & exporters endobj
InChI=1S/C10H12N2O4/ c1-3-16-10-5-4-8(11-7(2)13)6-9(10)12(14) 15/h4-6H,3H2,1-2H3,(H,11,13) … {�1%y��R�����m�4��
�l����M����Lf�Q�����N��~XRʟ?[�=��ӿ��,u'���'��u�ȍ���ϖ������ס7"7���? PubChem Substance ID 57652699. Main Uses: Organic dyes and pigments intermediates. Data compiled by: Coblentz Society, Inc. <<
The resulting thick dark solution was cooled and stored overnight in a refrigerator, followed by filtration. Visit our website to find more information like suppliers, MSDS, infra-red (IR), nuclear magnetic resonance spectra (NMR), bp, mp, nd20, molecular formula (MF), molfile, sdf file, structure, 3d model. Our Services. Molbase Encyclopedia provides phenacetin (62-44-2) basic information, physical and chemical properties, safety information, toxicity, customs data, synthetic routes, maps, MSDS, generation methods and uses, and its upstream and downstream products, … The component in the mixture includes 9 possible compounds (p-acetophenetidide, benzhydrol, biphenyl, 2'-bromoacetanilide, 4'-bromoacetanilide, caffine, phenylacetic acid, propyl 4-hydroxybenzoate, triphenylmethane) Please identify the major and minor component in the sample. %PDF-1.4
46 of 52 HCC patients (88.4%) had an abnormal phenacetin test before TACE, where the ratio of plasma total … Washing with ethanol, then ethanol/water solution and dried. Headquartered in Calgary, Canada, we are an NMR company that manufactures industry-leading portable desktop NMR instruments for a variety of applications across many market sectors, including teaching, biotech and pharma, polymer research, food science, synthetic chemistry, reaction … }�~N��*[^�����wI7�>�?�?��j����B����%�y8s}�R�8a�qA5nr�B���������V�_.��U�]P(�>ϖ�7�σ݃{�i�Hc8�M3��y��#��H!�β�w��v|�N�g?�s7�S��&�{�!~�7��f]o�W�zgp��'��Px���}(qO����Y�c@6E��02��Y�0�{�aߠG�Dyx���gO}H?� �����}��ww��}r6v�;���o-4b�-I��C�MN`�e�;�����I��B���m?�|���I��U}��s]�����_��!�7����Bw��fW��=�`�d�a������M���ߗ����g�� �w|���2�L��������齇=�� �����o�Ox������ν�{���ҽ}Z� i������DH�����}�7�����76��g������|J�_? p-Acetophenetidide Revision Date 19-Jan-2018 United States of America Inventory Component CAS-No TSCA TSCA Inventory notification - Active/Inactive TSCA - EPA Regulatory Flags Phenacetin 62-44-2 X ACTIVE S Legend: TSCA - Toxic Substances Control Act, (40 CFR Part 710) X - Listed '-' - Not Listed S - Indicates a substance that is identified in a proposed or final Significant New … In lab you will be provided with melting point and TLC standard samples of each of the possible compounds for comparison. spectra of carboxylic acid derivatives. D), and oxygen-17 (subvol. Explain about splitting, integration, shift for NMR table. (62-44-2) (N-12745-1G) 1.Certificate Of Analysis (COA) 2.Material Safety Data Sheet (MSDS) 3.Route of synthesis (ROS) 4.Method of Aanlysis (MOA) 5.Nuclear Magnetic Resonance (NMR) … C), carbon-13 (subvol. Home>Encyclopedia> “p-acetophenetidide, 2&#39; ... Properties Safety and Handling Reach Info MSDS NMR Spectrum Synthesis Route Precursor and Product Computational chemical data 560 Suppliers. �cB�7pF��*t��F��`��6��|��%g��M9���qv�(�s��]=�u���Q�=�%��;�߫� pzE�}'5q��.S��L_�7�!y;����g}��2W�dn�-;^��}�n(�/;rә��i�\�����l�S���� �foa��mX'Z:�n��qh�B����,���{�ɾz�a��U�O}��ῇI�9n�wB0�?w�?���9��j����c��hM-��Į_ʟf4��wC����~7B��;mG�?8��t]W����\q����Y�O�}��^US�q�vH����������}p�?�ګ~ܿǀ�o�We��
��3�c�{ё�m���A��l����7T��y4�������sog�����^��j�����ȭ^�t�y8?,���_ X�=�0��������̽��u�s�?����o�~�����78{���7y9�z���( ߰x�� %p���Ο�v�pI�����tx��J���GaU>�>|;��y�C����b��ځ��Ο�k�m������Ώ�h��;Я�0����K�<=�.xf�ҽ}����|g���j��tu�ӇL�q���Y=�}����NZ��e[�Ӭ-�����{���N��YH�N���g����:i�N/�77'���������O��S�g�ގ��kg"N�Ã{b�Q�cd��+��*tr;`:�iǑ
;y��(����9�� ��me�w���ס^�?�D���N/��vM������_�!|������÷�O�u��oCH����T��t�`g�:����3��}� Chemical shifts and coupling constants of boron-11 and phosphorus-31 (subvol. Acetaminophen relieves pain by raising the body’s pain threshold, and it reduces fever by its action on the temperature-regulating centre of the brain. SMILES. Identification 1.1 GHS … The component in the mixture includes 9 possible compounds (p-acetophenetidide, benzhydrol, biphenyl, 2'-bromoacetanilide, 4'-bromoacetanilide, caffine, phenylacetic acid, propyl 4-hydroxybenzoate, triphenylmethane) Please identify the major and minor component in the sample. Shop a large selection of Benzene and substituted derivatives products and learn more about 4-Acetophenetidide, 97%, ACROS Organics™ . ;�wǁ���2����i��6d��B�;�Q*�h�{���~:��C�R�O�e:�n���͐KC��L�Y�u��R� �l4�cL����mg����6$Rg4>{���}8���Eض�m�kGl:H�|]�ǘ���� �,�Ô�? Molecular Weight 179.22 . Synonym: 1-Acetyl-p-phenetidin, 4′-Ethoxyacetanilide, N-(4-Ethoxyphenyl)acetamide, p-Acetophenetidide, Acetophenetidin, Phenacetin Linear Formula: CH 3 CONHC 6 H 4 OC 2 H 5 Molecular Weight: 179.22 For the experiments in the last section of this paper, probe temperatures weremeasured with a calibrated Eurotherm 840/T digital thermometer, connected to a thermocouple which was introduced into an NMR … Compared with normal controls, phenacetin apparent clearance decreased by 47.0% (p < 0.05) and 78.7% (p < 0.01) in patients with chronic hepatitis B and cirrhosis, respectively. Go To: Top, References, Notes Data compilation copyrightby the U.S. Secretary of Commerce on behalf of the U.S.A.All rights reserved. III. o|?{z#r�{����ܝ? Results: NMR spectra were analyzed to narrow down the possible compounds in the unknown #77 mixture. <>
: 122-82-7: EINECS NO: 204-577-1: Formula: C 12 H 15 NO 3: Structure Formula: M.W.： 221.25: Characters: White crystalline powder. InChi. Chemical Formula: C 10 H 13 NO 2. click here for … The recovery of phenacetin O-de-ethylated metabolites decreased by 24.6 and 72.4% (p < 0.01). Resources Search for: p-Acetophenetidide . Molecular Formula C 10 H 12 N 2 O 4; Average mass 224.213 Da; Monoisotopic mass 224.079712 Da; ChemSpider ID 14919; More details: Systematic name. Linear Formula CH 3 CONHC 6 H 4 OC 2 H 5. CAS Number: 62-44-2 . Imidacloprid. 4 0 obj
p-Acetophenetidine - chemical information, properties, structures, articles, patents and more chemical data. P-acetophenetidide will be in the organic layer. ;�j �D�i���(�n�c��0��mX����Q�æ��ف��mۍ���� ��y1��i�q���ľO���'���PH�் Based on the components of your mixture, you will need to decide which method to use. Correlation of 13C N.M.R. Std. NMR spectra were taken in a Bruker DPX-300 instrument (300.1 and 75.5 MHz for 1Hand13C, respectively). Tags:p-Acetotoluidide(103-89-9) 1 H NMR Related Products. >>
p-Acetophenetidide 2 (1.79 g,0.1 mol), malononitrile (6.96 g, 0.1 mol), and sulfur (3.37 g, 0.1 mol) in ethanol were stirred in the presence of morpholine (8.97g, 0.1 mol) at 60-70°C for 3 hrs. Unless otherwise indicated, all were run at room temperature (24 ( 1 °C). Explain about splitting, integration, shift for NMR table. Names and Identifiers Properties Safety and Handling NMR Spectrum Synthesis Route Precursor and Product Computational chemical data 261 Suppliers. A), fluorine-19 and nitrogen-15 (subvol. 1. 1 0 obj
p-Acetylamino benzoic acid(556-08-1) 13 CNMR p-Acetylamino benzoic acid(556-08-1) 1 HNMR p-Acetylamino benzoic acid(556-08-1)IR1 p-Acetylamino benzoic acid(556-08-1)Raman Acetoacetanilide(102-01-2)MS Acetoacetanilide(102-01-2) 13 CNMR Acetoacetanilide(102-01-2)Raman Acetoacetanilide(102-01-2)IR2 Acetoacetanilide(102-01-2) … • p-acetophenetidide ... You will be given NMR spectra for your compounds to help with confirmation of your unknown identities. This was compared to mixed melting points of the standards provided of p View the Full Spectrum for FREE! Creation Date: Aug 17, 2017. Also, please choose one method to separate … EC Number 200-533-0. 90+% BY 1H NMR: Last updated: last month: In warehouse: Unverified Salt: free: Pack size Ships out Price Qty; 1 mg February 23, 2021 15.00 USD: ADD TO CART: 5 mg February 23, 2021 25.00 USD: ADD TO CART: 10 mg February 23, 2021 30.00 USD: ADD TO CART: 15 mg February 23, 2021 35.00 USD: ADD TO CART: 20 mg February 23, 2021 40.00 USD: ADD TO CART: 25 mg February 23, … Bioaccumulation Estimates from Log Kow (BCFWIN v2.17): Log BCF from regression-based method = 0.332 (BCF = 2.147) log Kow used: 1.34 (expkow database) Volatilization from Water: Henry LC: 2.46E-009 atm-m3/mole (estimated by Bond SAR Method) Half-Life from Model River: 3.482E+005 hours (1.451E+004 days) Half-Life from Model Lake : 3.799E+006 hours (1.583E+005 days) Removal In … Revision Date: Aug 17, 2017. IUPAC Name: N-(4-ethoxyphenyl)acetamide . SAFETY DATA SHEETS According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition. This database is a catalog of over 1500000 chemicals and over 1000 chemical suppliers. Minor Product: Discussion: Before any experiments were conducted, NMR was used to narrow down the possible compounds of the mixture. 3-NITRO-P-ACETOPHENETIDIDE. Beilstein/REAXYS Number 1869238 . Yield 73%, mp 292-294°C. Phenylacetic acid is a monocarboxylic acid that is toluene in which one of the hydrogens of the methyl group has been replaced by a carboxy group. P-acetophenetidide, 2-bromoacetanilide, and propyl 4-hydroxybenzoate were the predicted possible compounds.Melting point was then used on the unknown. '.|�6�8�f��!�N�@"}}���[A���v��|�a��&H�%����{����h�\��>�w��������wh�C�u21aӸ�Ы��������o����0��w�__ۂ�f�R����uq�����U=��c�v����>�fˋ�� ��!�j�.�`��4�Mѽ�Oٓ�L�PyvlH��ӱ(���B0a�л�ڈk�c�W�u E��o��.}�]��l����r��KƧ�? p-Acetophenetidide: CAS No. B), hydrogen-1 (subvol. 17O NMR studies on substitutedN-arylacetamides and aryl acetates: Torsion angle and electronic effects Magnetic Resonance in Chemistry: 1988: Substituent effects on the N.M.R. stream
Phenacetin (acetophenetidin, N- (4-ethoxyphenyl)acetamide) is a pain-relieving and fever-reducing drug, which was widely used following its introduction in 1887. Version: 1.0. The full spectrum can only be viewed using a FREE account. List of all Manufacturers, Suppliers & Exporters of 1-Acetyl-p-phenetidin; 4 inverted exclamation marka-Ethoxyacetanilide; N-(4-Ethoxyphenyl)acetamide; p-Acetophenetidide; Acetophenetidin API listed on PharmaCompass with details of regulatory filings All Rights Reserved, 4-13-00-01092 (Beilstein Handbook Reference), Phenacetin [Analgesic mixtures containing phenacetin]. CAS No: 138261-41-3; Molecular Weight: 255.661; Molecular Formula:C 9 H 10 CLN 5 O 2; Boiling Point:411.7°C at 760 mmHg; Melting Point:144℃ Properties Safety and Handling … After separating the layers, the compounds can be extracted and tested for its identify through melting point. Abstract: This volume provides a comprehensive and evaluated compilation of nuclear magnetic resonance data. X���`I�%&/m�{J�J��t��`$ؐ@������iG#)�*��eVe]f@�흼��{���{���;�N'���?\fdl��J�ɞ!���?~|? Synonym: 1-Acetyl-p-phenetidin, 4′-Ethoxyacetanilide, N-(4-Ethoxyphenyl) acetamide, p-Acetophenetidide, Acetophenetidin CAS Number 62-44-2. SDS. MDL number MFCD00009094. Nanalysis Corp. is the world-leading manufacturer of compact, portable, benchtop NMR spectrometers. • p-acetophenetidide ... You will then be given NMR spectra for your compounds to help with confirmation of your unknown identities. It was withdrawn from medicinal use as dangerous from the 1970s (e.g., withdrawn in Canada in 1973, and by the U.S. Food and Drug Administration in 1983). NACRES NA.22 Other articles where Acetophenetidin is discussed: acetaminophen: …major metabolite of acetanilid and phenacetin, which were once commonly used drugs, and is responsible for their analgesic (pain-relieving) effects. You will also find information like safety, risk, hazard and MSDS. N-(4-Ethoxy-3-nitrop henyl)acetamide. The 82 MHz spectrum of a 6% (w/w; 0.5 M) solution of phenacetin in CDCl 3 acquired using the Thermo Scientific picoSpin 80 NMR spectrometer. "R}~Q:~pgg'������"���l���/���������O�:OϽV�ޞ�~
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